dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

Base Information

Chemical Name:dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate
CAS No.:1262030-04-5
Molecular Formula:C₁₀H₁₄N₂O₆
Molecular Weight:258.231
Hs Code.:

Synonyms:dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

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Chemical Property of dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

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Technology Process of dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

There total 3 articles about dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 6832-16-2
methyl diazoacetate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: scandium tris(trifluoromethanesulfonate)

: 19255-80-2
5-methoxycarbonyl-pyrazoline-3-carboxylic acid methyl ester

: 1262030-04-5
dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

: 88016-31-3
(trifluoromethanesulfonyloxy)acetic acid methyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1007/s11172-010-0194-0

Reference yield: 35.0%

: tin(II) trifluoromethanesulfonate

: 6832-16-2
methyl diazoacetate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 19255-80-2
5-methoxycarbonyl-pyrazoline-3-carboxylic acid methyl ester

: 1262030-04-5
dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

: 88016-31-3
(trifluoromethanesulfonyloxy)acetic acid methyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1007/s11172-010-0194-0

Reference yield: 15.0%

: 6832-16-2
methyl diazoacetate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 19255-80-2
5-methoxycarbonyl-pyrazoline-3-carboxylic acid methyl ester

: 1262030-04-5
dimethyl 1-(2-methoxy-2-oxoethyl)-4,5-dihydro-1H-pyrazole-3,5-dicarboxylate

: 96-34-4
methyl chloroacetate

Guidance literature:: With gallium(III) trichloride; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1007/s11172-010-0194-0