4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

Base Information

Chemical Name:4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide
CAS No.:122924-18-9
Molecular Formula:C₄₆H₅₄BrNO₁₆
Molecular Weight:956.836
Hs Code.:

4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

Synonyms:4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

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Chemical Property of 4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

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Technology Process of 4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

There total 6 articles about 4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106989-01-9
1L-2-azido-1,4,5,6-tetra-O-benzyl-2-desoxy-4-C-(benzyloxymethyl)-muco-inosit

: 122924-18-9
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / NaBH₄ / 4 percent NiCl₂ / ethanol

2: propan-1-ol / 30 h / 90 °C

3: pyridine

4: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

5: 157 mg / HBr / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen bromide; nickel dichloride; In propan-1-ol; ethanol; dichloromethane;

Reference yield:

: 122901-35-3,122999-53-5
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

: 122924-18-9
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

Guidance literature:: With hydrogen bromide; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 33208-46-7
1,6:3,4-Dianhydro-2-O-benzyl-β-D-galactopyranose

: 122924-18-9
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: propan-1-ol / 30 h / 90 °C

2: pyridine

3: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

4: 157 mg / HBr / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; hydrogen bromide; In propan-1-ol; dichloromethane;