bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate

Base Information

Chemical Name:bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate
CAS No.:1099824-63-1
Molecular Formula:C₂₃H₂₅F₆NO₇
Molecular Weight:541.444
Hs Code.:

Synonyms:bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate

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Chemical Property of bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate

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Technology Process of bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate

There total 2 articles about bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 407-47-6,29036-64-4
2,2,2-trifluoroethyl acrylate

: 634902-31-1
4-methoxy-1-(4-methoxybenzyl)-2,5-dihydro-1H-2-azolone

: 1099824-63-1
bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at -25 ℃; for 6h;
DOI:10.1016/j.tet.2008.10.007

Reference yield: 19.0%

: 407-47-6,29036-64-4
2,2,2-trifluoroethyl acrylate

: 634902-31-1
4-methoxy-1-(4-methoxybenzyl)-2,5-dihydro-1H-2-azolone

: 1099824-62-0
2,2,2-trifluoroethyl 3-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrol-2-yl]propanoate

: 1099824-63-1
bis(2,2,2-trifluoroethyl) 3,3'-[1-(4-methoxybenzyl)-2,5-dihydro-3-methoxy-5-oxo-1H-pyrrole-2,2-diyl]dipropanoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at -30 ℃; for 6h;
DOI:10.1016/j.tet.2008.10.007