2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

Base Information

Chemical Name:2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate
CAS No.:1294451-57-2
Molecular Formula:C₁₇H₁₄ClF₄N₃O₄
Molecular Weight:435.762
Hs Code.:

Synonyms:2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

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Chemical Property of 2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

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Technology Process of 2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

There total 4 articles about 2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1069042-33-6
2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

: 108-24-7
acetic anhydride

: 1294451-57-2
2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 48h;
DOI:10.3184/030823410X12890538073580

Reference yield:

: 1069042-30-3
3-(4-chloro-6-fluoro-3-methoxy-2-nitrophenyl)-1-methyl-5-trifluoromethyl-1H-pyrazole

: 1294451-57-2
2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 20 °C

2: iron; ammonium chloride / methanol; water / 6 h / 55 °C / Inert atmosphere

3: triethylamine / toluene / 48 h / 20 °C

With aluminum (III) chloride; iron; ammonium chloride; triethylamine; In methanol; dichloromethane; water; toluene;
DOI:10.3184/030823410X12890538073580

Reference yield:

: 1069042-32-5
6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-2-nitrophenol

: 1294451-57-2
2-(N-acetylacetamido)-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride / methanol; water / 6 h / 55 °C / Inert atmosphere

2: triethylamine / toluene / 48 h / 20 °C

With iron; ammonium chloride; triethylamine; In methanol; water; toluene;
DOI:10.3184/030823410X12890538073580