2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

Base Information

Chemical Name:2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol
CAS No.:1069042-33-6
Molecular Formula:C₁₁H₈ClF₄N₃O
Molecular Weight:309.651
Hs Code.:

Synonyms:2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

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Technology Process of 2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

There total 3 articles about 2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1069042-32-5
6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-2-nitrophenol

: 1069042-33-6
2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

Guidance literature:: With iron; ammonium chloride; In methanol; water; at 55 ℃; for 6h; Inert atmosphere;
DOI:10.3184/030823410X12890538073580

Reference yield:

: 1069042-30-3
3-(4-chloro-6-fluoro-3-methoxy-2-nitrophenyl)-1-methyl-5-trifluoromethyl-1H-pyrazole

: 1069042-33-6
2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 20 °C

2: iron; ammonium chloride / methanol; water / 6 h / 55 °C / Inert atmosphere

With aluminum (III) chloride; iron; ammonium chloride; In methanol; dichloromethane; water;
DOI:10.3184/030823410X12890538073580

Reference yield:

: 142623-41-4
3-(4-chloro-2-fluoro-5-methoxyphenyl)-1-methyl-5-trifluoromethyl-1H-pyrazole

: 1069042-33-6
2-amino-6-chloro-4-fluoro-3-(1-methyl-5-trifluoromethyl-1H-pyrazol-3-yl)-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; acetic anhydride; acetic acid / 2 h / 0 °C

2: aluminum (III) chloride / dichloromethane / 2 h / 20 °C

3: iron; ammonium chloride / methanol; water / 6 h / 55 °C / Inert atmosphere

With aluminum (III) chloride; nitric acid; acetic anhydride; iron; ammonium chloride; acetic acid; In methanol; dichloromethane; water;
DOI:10.3184/030823410X12890538073580