1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

Base Information

Chemical Name:1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide
CAS No.:89409-30-3
Molecular Formula:C₂₉H₂₅ClNS₂*I
Molecular Weight:614.014
Hs Code.:

Synonyms:1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

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Chemical Property of 1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

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Technology Process of 1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

There total 1 articles about 1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 89409-12-1
1-(4-Chloro-phenyl)-2,4-diphenyl-1,5,6,7-tetrahydro-quinoline

: 74-88-4
methyl iodide

: 89409-43-8
8--1-(4-chlorophenyl)-2-4-diphenyl-5,6,7,8-tetrahydroquinolinium iodide

: 89409-30-3
1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given; 1.) -10 deg C --> room temperature, 30 min, 2.) -10 deg C --> room temeorature, 2 h;
DOI:10.1039/P19830002605

Reference yield: 95.0%

: 89409-30-3
1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

: 89409-35-8
1-(4-Chloro-phenyl)-2,4-diphenyl-1,5,6,7-tetrahydro-quinoline-8-carbodithioic acid methyl ester

Guidance literature:: With sodium ethanolate; In ethanol; for 0.5h;
DOI:10.1039/P19830002605

Reference yield:

: 89409-30-3
1-(4-Chloro-phenyl)-8-methylsulfanylthiocarbonyl-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; iodide

: 89409-40-5
8-[1-(4-Chloro-phenylsulfanyl)-1-methylsulfanyl-meth-(Z)-ylidene]-2,4-diphenyl-5,6,7,8-tetrahydro-quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium ethoxide / ethanol / 0.5 h

2: 90 percent / toluene / 20 h / Heating

With sodium ethanolate; In ethanol; toluene;
DOI:10.1039/P19830002605