Technology Process of 8-<4-(2-Hydroxyethyl)phenyl>naphthalin-1-carboxamidoxim
There total 8 articles about 8-<4-(2-Hydroxyethyl)phenyl>naphthalin-1-carboxamidoxim which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; triethylamine;
In
diethyl ether;
for 69h;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / BH3*Me2S / diethyl ether / 2.5 h / Heating
2: 99 percent / pyridinium-p-toluene-sulfonate / CH2Cl2 / 3 h
4: conc. HCl / methanol; H2O / 2 h / Ambient temperature
5: 30 percent / NH2OH*HCl, triethylamine / diethyl ether / 69 h / Heating
With
hydrogenchloride; dimethylsulfide borane complex; hydroxylamine hydrochloride; pyridinium p-toluenesulfonate; triethylamine;
In
methanol; diethyl ether; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / pyridinium-p-toluene-sulfonate / CH2Cl2 / 3 h
3: conc. HCl / methanol; H2O / 2 h / Ambient temperature
4: 30 percent / NH2OH*HCl, triethylamine / diethyl ether / 69 h / Heating
With
hydrogenchloride; hydroxylamine hydrochloride; pyridinium p-toluenesulfonate; triethylamine;
In
methanol; diethyl ether; dichloromethane; water;
