3-(p-Chlorophenyl)-2-oxo-5-oxazolidinylmethyl=carbamate

Base Information

• Chemical Name: 3-(p-Chlorophenyl)-2-oxo-5-oxazolidinylmethyl=carbamate
• CAS No.: 29218-31-3
• Molecular Formula: C₁₁H₁₁ClN₂O₄
• Molecular Weight: 270.672
• Hs Code.: 2934999090
• Mol file: 29218-31-3.mol

Synonyms:2-Oxazolidinone,3-(p-chlorophenyl)-5-(hydroxymethyl)-, carbamate (ester) (8CI)

Chemical Property of 3-(p-Chlorophenyl)-2-oxo-5-oxazolidinylmethyl=carbamate

Chemical Property:

• Vapor Pressure: 4.55E-09mmHg at 25°C
• Boiling Point: 471.7°Cat760mmHg
• Flash Point: 239.1°C
• PSA: 82.85000
• Density: 1.438g/cm³
• LogP: 2.33930

Purity/Quality:

3-(P-CHLOROPHENYL)-5-HYDROXYMETHYL-2-OXAZOLIDINONE CARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(p-Chlorophenyl)-2-oxo-5-oxazolidinylmethyl=carbamate

There total 2 articles about 3-(p-Chlorophenyl)-2-oxo-5-oxazolidinylmethyl=carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-chloro-N-(2,3-dihydroxypropyl)-aniline (42902-60-3) → 5-carbamoyloxymethyl-3-(4-chloro-phenyl)-oxazolidin-2-one (29218-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i), (ii) NaOMe, MeOH

2: (i) PhNEt₂, toluene, (ii) NH₃, benzene

Reference yield:

phosgene (75-44-5) + 5-hydroxymethyl-3-p-chlorophenyl-oxazolidin-2-one (29218-25-5) → 5-carbamoyloxymethyl-3-(4-chloro-phenyl)-oxazolidin-2-one (29218-31-3)

Guidance literature:

Multistep reaction; (i) PhNEt₂, toluene, (ii) NH₃, benzene;

upstream raw materials:

phosgene

5-hydroxymethyl-3-p-chlorophenyl-oxazolidin-2-one

p-chloro-N-(2,3-dihydroxypropyl)-aniline

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