C₄₈H₄₆N₂O₈S₄

Base Information

Chemical Name:C₄₈H₄₆N₂O₈S₄
CAS No.:1383942-54-8
Molecular Formula:C₄₈H₄₆N₂O₈S₄
Molecular Weight:907.166
Hs Code.:

C<sub>48</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>S<sub>4</sub>

Synonyms:C₄₈H₄₆N₂O₈S₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₄₆N₂O₈S₄

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Technology Process of C₄₈H₄₆N₂O₈S₄

There total 5 articles about C₄₈H₄₆N₂O₈S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1383942-34-4
C₄₅H₄₅NO₇S₄

: 372-09-8
cyanoacetic acid

: 1383942-54-8
C₄₈H₄₆N₂O₈S₄

Guidance literature:: With piperidine; acetic acid; In chloroform; for 12h; Reflux;
DOI:10.1016/j.tet.2012.04.113

Reference yield:

: 3807-53-2
dithieno[3,2-b:2′,3′-d]thiophene-4,4-dioxide

: 1383942-54-8
C₄₈H₄₆N₂O₈S₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 25.5 h / 15 - 20 °C / Darkness

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 24 h / Inert atmosphere; Reflux

3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h / 20 °C / Darkness

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 5 h / Inert atmosphere; Reflux

5.1: trichlorophosphate / 1 h / 0 °C

5.2: 1 h / 0 - 20 °C

5.3: pH 10

6.1: piperidine; acetic acid / chloroform / 12 h / Reflux

With piperidine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; trichlorophosphate; In chloroform; para-xylene; N,N-dimethyl-formamide; 2.1: Stille coupling / 4.1: Stille coupling / 5.2: Vilsmeier-Haack reaction / 6.1: Knoevenagel condensation;
DOI:10.1016/j.tet.2012.04.113

Reference yield:

: 1383942-30-0
C₃₈H₄₁NO₄S₃

: 1383942-54-8
C₄₈H₄₆N₂O₈S₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h / 20 °C / Darkness

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 5 h / Inert atmosphere; Reflux

3.1: trichlorophosphate / 1 h / 0 °C

3.2: 1 h / 0 - 20 °C

3.3: pH 10

4.1: piperidine; acetic acid / chloroform / 12 h / Reflux

With piperidine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; trichlorophosphate; In chloroform; para-xylene; N,N-dimethyl-formamide; 2.1: Stille coupling / 3.2: Vilsmeier-Haack reaction / 4.1: Knoevenagel condensation;
DOI:10.1016/j.tet.2012.04.113