methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

Base Information

Chemical Name:methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride
CAS No.:914835-64-6
Molecular Formula:C₂₃H₂₂N₂O₃*ClH
Molecular Weight:410.9
Hs Code.:

Synonyms:methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

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Chemical Property of methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

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Technology Process of methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

There total 7 articles about methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 914835-51-1
1-t-butyl 2-methyl (2S,4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]pyrrolidine-1,2-dicarboxylate

: 914835-64-6
methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 2h;

Reference yield:

: 914835-38-4
1-t-butyl 2-methyl (2S,4R)-4-[(6-bromo-2-phenylquinolin-4-yl)oxy]pyrrolidine-1,2-dicarboxylate

: 914835-64-6
methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 3 h / 110 °C

2: hydrogenchloride / 1,4-dioxane / 2 h

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; toluene;

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 914835-64-6
methyl (4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: PPA / 3 h / 150 °C

1.2: 20 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 5 h / 45 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 3 h / 110 °C

4.1: hydrogenchloride / 1,4-dioxane / 2 h

With hydrogenchloride; PPA; caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; toluene;