Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

Base Information

Chemical Name:Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester
CAS No.:192657-40-2
Molecular Formula:C₂₄H₂₈N₂O₆S₂
Molecular Weight:504.628
Hs Code.:

Synonyms:Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

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Chemical Property of Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

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Technology Process of Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

There total 1 articles about Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112089-53-9
5-(benzyloxy)-1,2,3,6,7,8-hexahydro-3-(methylsulfonyl)-8-(methylthio)-7-oxobenzo[1,2-b:4,3-b']dipyrrole-1-methanol acetate

: 74-88-4
methyl iodide

: 192657-40-2
Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja9703133

Reference yield:

: 192657-40-2
Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

: 192657-41-3
(5-Benzyloxy-3-methanesulfonyl-6,8-dimethyl-1,2,3,6-tetrahydro-pyrrolo[3,2-e]indol-1-yl)-methanol

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; Yield given;
DOI:10.1021/ja9703133

Reference yield:

: 192657-40-2
Acetic acid 5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-8-methylsulfanyl-7-oxo-1,2,3,6,7,8-hexahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

: 192657-42-4
(S)-2-tert-Butoxycarbonylamino-3-(1H-indol-3-yl)-propionic acid (S)-5-benzyloxy-3-methanesulfonyl-6,8-dimethyl-1,2,3,6-tetrahydro-pyrrolo[3,2-e]indol-1-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: BH₃*(CH₃)2S / tetrahydrofuran

2: DCC, N-methylimidazole / dioxane

With 1-methyl-1H-imidazole; dimethylsulfide borane complex; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ja9703133