(-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

Base Information

Chemical Name:(-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose
CAS No.:1332506-93-0
Molecular Formula:C₁₁H₁₁FO₂
Molecular Weight:194.206
Hs Code.:

Synonyms:(-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

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Technology Process of (-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

There total 2 articles about (-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1332506-86-1
(-)-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

: 1332506-93-0
(-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

Guidance literature:: With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo201110z

Reference yield:

: 1332506-77-0
(2R,1'S)-tert-butyl(dimethyl)(2-(1'-(3''-fluorophenyl)allyloxy)-but-3-enyloxy)silane

: 1332506-93-0
(-)-2',3'-didehydro-1',2',3'-trideoxy-1'-(3-fluorophenyl)-β-L-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs catalyst first generation / dichloromethane / 5 h / 40 °C / Inert atmosphere

2: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C / Inert atmosphere

With Grubbs catalyst first generation; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo201110z