1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

Base Information

Chemical Name:1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate
CAS No.:153959-43-4
Molecular Formula:C₃₈H₅₈ClO₁₀P
Molecular Weight:741.299
Hs Code.:

Synonyms:1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

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Chemical Property of 1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

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Technology Process of 1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

There total 8 articles about 1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 505-95-3
12-hydroxydodecanoic acid

: 153959-43-4
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / Et₃N / ethyl acetate / 12 h / Heating

2: 60.6 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

3: NaH / hexane; tetrahydrofuran / 28 h

4: TBAF / tetrahydrofuran / 0.75 h

5: pyridine / tetrahydrofuran / 4 h

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; hexane; chloroform; ethyl acetate;
DOI:10.1021/jo00082a009

Reference yield:

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 153959-43-4
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / Et₃N / ethyl acetate / 12 h / Heating

2: 60.6 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

3: NaH / hexane; tetrahydrofuran / 28 h

4: TBAF / tetrahydrofuran / 0.75 h

5: pyridine / tetrahydrofuran / 4 h

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; hexane; chloroform; ethyl acetate;
DOI:10.1021/jo00082a009

Reference yield:

: 153959-38-7
2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

: 153959-43-4
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-2-O-methyl-sn-glyceryl o-chlorophenyl 2',3'-isopropylidene-sn-glyceryl phosphate

Guidance literature:: Multi-step reaction with 4 steps

1: 60.6 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

2: NaH / hexane; tetrahydrofuran / 28 h

3: TBAF / tetrahydrofuran / 0.75 h

4: pyridine / tetrahydrofuran / 4 h

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; hexane; chloroform;
DOI:10.1021/jo00082a009