methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

Base Information

Chemical Name:methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate
CAS No.:94103-09-0
Molecular Formula:C₂₄H₃₀INO₇
Molecular Weight:571.409
Hs Code.:

Synonyms:methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

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Technology Process of methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

There total 9 articles about methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 94103-04-5
methyl 2-methoxy-4-(5-methoxy-4-nitro-3-propylphenoxy)-6-pentylbenzoate

: 94103-09-0
methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

Guidance literature:: With iodine; silver trifluoroacetate; In chloroform;

Reference yield:

: 1700-37-4
3-Benzyloxybenzaldehyde

: 94103-09-0
methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) magnesium / 1.) diethyl ether, 2.) 0 deg C (1 h), room temperature (1 h), reflux (1 h)

2: 81 percent / hydrogen, hydrochloric acid / palladized charcoal / acetic acid

3: 75 percent / bromine, aluminium powder

4: 93 percent / aluminium chloride / benzene / 0.5 h / Heating

5: 24 percent / nitric acid / acetic acid / 10 - 15 °C

6: potassium carbonate / dimethylformamide / Ambient temperature

7: 67 percent / potassium carbonate, pyridine, copper(II) oxide / 18 h / 140 °C

8: 100 percent / iodine, silver trifluoroacetate / CHCl₃

With pyridine; hydrogenchloride; aluminium trichloride; hydrogen; bromine; iodine; nitric acid; silver trifluoroacetate; potassium carbonate; magnesium; aluminium; copper(II) oxide; palladium on activated charcoal; In chloroform; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 55789-02-1
α-ethyl-3-hydroxybenzyl alcohol

: 94103-09-0
methyl 5-iodo-4-(5-methoxy-4-nitro-3-propylphenoxy)-2-methoxy-6-pentylbenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / hydrogen, hydrochloric acid / palladized charcoal / acetic acid

2: 75 percent / bromine, aluminium powder

3: 93 percent / aluminium chloride / benzene / 0.5 h / Heating

4: 24 percent / nitric acid / acetic acid / 10 - 15 °C

5: potassium carbonate / dimethylformamide / Ambient temperature

6: 67 percent / potassium carbonate, pyridine, copper(II) oxide / 18 h / 140 °C

7: 100 percent / iodine, silver trifluoroacetate / CHCl₃

With pyridine; hydrogenchloride; aluminium trichloride; hydrogen; bromine; iodine; nitric acid; silver trifluoroacetate; potassium carbonate; aluminium; copper(II) oxide; palladium on activated charcoal; In chloroform; acetic acid; N,N-dimethyl-formamide; benzene;