2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

Base Information

Chemical Name:2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide
CAS No.:930806-07-8
Molecular Formula:C₃₄H₄₂N₄O₁₃
Molecular Weight:714.726
Hs Code.:

Synonyms:2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

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Chemical Property of 2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

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Technology Process of 2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

There total 2 articles about 2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₁₉H₂₂O₈C₆H₁₂O₄N₄C₂H₂OC₃H₄C₇H₆

: 930806-07-8
2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

Guidance literature:: C₁₉H₂₂O₈C₆H₁₂O₄N₄C₂H₂OC₃H₄C₇H₆; With hydrogen; [Ir(I)(cycloocta-1,5-diene)(PmePh₂)2]PF₆; In tetrahydrofuran;

With toluene-4-sulfonic acid; In methanol; Further stages.;
DOI:10.1002/anie.200604442

Reference yield: 74.0%

: 2-acetamido-3-O-allyloxycarbonyl-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

: 930806-07-8
2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2006.09.012

Reference yield: 69.0%

: 930806-07-8
2-acetamido-4-O-(6''-O-benzyl-2'',3'',4''-tri-O-acetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-β-D-glucopyranosyl azide

: 169532-17-6,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-α/β-L-fucopyranoside

: 2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(2'',3'',4''-tri-O-acetyl-6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

Guidance literature:: With tetrabutylammomium bromide; copper(ll) bromide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1016/j.carres.2006.09.012