N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Base Information

Chemical Name:N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide
CAS No.:1432514-50-5
Molecular Formula:C₁₈H₁₆N₄O₆S₂
Molecular Weight:448.48
Hs Code.:

Synonyms:N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Suppliers and Price of N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

There total 3 articles about N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27685-90-1
2-oxo-2,3-dihydrobenzo[d]oxazole-6-sulfonyl chloride

: 1063733-41-4
N-[(2,4-dimethoxyphenyl)methyl]-1,2,4-thiadiazol-5-amine

: 1432514-50-5
N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Guidance literature:: N-[(2,4-dimethoxyphenyl)methyl]-1,2,4-thiadiazol-5-amine; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 25 ℃;

2-oxo-2,3-dihydrobenzo[d]oxazole-6-sulfonyl chloride; In tetrahydrofuran; at -78 - 25 ℃;

Reference yield:

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 1432514-50-5
N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 2 h / Reflux; Dean-Stark

2.1: sodium tetrahydroborate / methanol / 0 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - 25 °C

3.2: -78 - 25 °C

With sodium tetrahydroborate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; toluene;

Reference yield:

: C₁₁H₁₁N₃O₂S

: 1432514-50-5
N-(2,4-dimethoxybenzyl)-2-oxo-N-(1,2,4-thiadiazol-5-yl)-2,3-dihydro-1,3-benzoxazole-6-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol / 0 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - 25 °C

2.2: -78 - 25 °C

With sodium tetrahydroborate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;