rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate

Base Information

Chemical Name:rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate
CAS No.:1075221-38-3
Molecular Formula:C₃₄H₃₄F₂N₂O₄
Molecular Weight:572.652
Hs Code.:

Synonyms:rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate

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Technology Process of rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate

There total 1 articles about rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₃₃N₅O₂

: 667-27-6
Ethyl bromodifluoroacetate

: 1075221-38-3
rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate

Guidance literature:: Ethyl bromodifluoroacetate; With chloro-trimethyl-silane; zinc; In tetrahydrofuran; for 0.166667h; Inert atmosphere;

C₃₆H₃₃N₅O₂; In tetrahydrofuran; at 60 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.200800363

Reference yield: 72.0%

: 1075221-38-3
rac-benzyl 4-[1-(dibenzylamino)-2-(ethoxycarbonyl)-2,2-difluoroethyl]benzylcarbamate

: 1075221-43-0
rac-ethyl 3-amino-3-[4-(aminomethyl)phenyl]-2,2-difluoropropanoate hydrochloride

Guidance literature:: With hydrogenchloride; 10% Pd/C; hydrogen; In ethanol; ethyl acetate; isopropyl alcohol; at 40 ℃; for 72h; under 760.051 Torr;
DOI:10.1002/ejoc.200800363