Technology Process of C19H30N6O4
There total 1 articles about C19H30N6O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium cyanoborohydride; acetic acid / 0 °C
2: methanol / 72 h / 65 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -15 - 20 °C
With
lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm300917h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
2: hydrazine hydrate / ethanol / 2 h / 80 °C
3: triethylamine / dichloromethane / 1 h / 20 °C
With
di-isopropyl azodicarboxylate; hydrazine hydrate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane;
1: |Mitsunobu Displacement;
DOI:10.1021/jm300917h
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
2: hydrazine hydrate / ethanol / 2 h / 80 °C
3: triethylamine / dichloromethane / 1 h / 20 °C
4: hydrogenchloride / 1,4-dioxane; methanol / 4 h
With
hydrogenchloride; di-isopropyl azodicarboxylate; hydrazine hydrate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane;
1: |Mitsunobu Displacement;
DOI:10.1021/jm300917h
