Technology Process of C29H31N5O4
There total 11 articles about C29H31N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
at 100 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide; water / ethanol / 2 h / Reflux
1.2: 16 h
2.1: methanol; diethyl ether / 1 h / 0 °C
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride / tetrahydrofuran; toluene / 24 h / Inert atmosphere; Reflux
4.1: hydrazine hydrate / 2 h / 100 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; hydrazine hydrate; cesium fluoride; potassium hydroxide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
1.2: 12 h / 65 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride / tetrahydrofuran; toluene / 24 h / Inert atmosphere; Reflux
3.1: hydrazine hydrate / 2 h / 100 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; hydrazine hydrate; cesium fluoride;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;