2-[(4-Cyclohexyl-2-ethylbutyl)amino]ethanethiol sulfate

Base Information

• Chemical Name: 2-[(4-Cyclohexyl-2-ethylbutyl)amino]ethanethiol sulfate
• CAS No.: 19142-97-3
• Molecular Formula: C14H29NO3S2
• Molecular Weight: 323.52
• Hs Code.: 2930909090
• Mol file: 19142-97-3.mol

Synonyms:S-2-(((4-Cyclohexyl-2-ethyl)butyl)amino)ethyl thiosulfate;2-(((4-Cyclohexyl-2-ethyl)butyl)amino)ethanethiol hydrogen sulfate (ester);s-{2-[(4-cyclohexyl-2-ethylbutyl)amino]ethyl} hydrogen sulfurothioate;Ethanethiol,2-((4-cyclohexyl-2-ethylbutyl)amino)-,hydrogen sulfate (ester);

Chemical Property of 2-[(4-Cyclohexyl-2-ethylbutyl)amino]ethanethiol sulfate

Chemical Property:

• PSA: 100.08000
• Density: 1.136g/cm³
• LogP: 4.97040

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[(4-Cyclohexyl-2-ethylbutyl)amino]ethanethiol sulfate

There total 4 articles about 2-[(4-Cyclohexyl-2-ethylbutyl)amino]ethanethiol sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexylacetaldehyde (5664-21-1) → Thiosulfuric acid S-[2-(4-cyclohexyl-2-ethyl-butylamino)-ethyl] ester (19142-97-3)

Guidance literature:

Multi-step reaction with 4 steps

1: zinc

2: sulfuric acid; toluene-4-sulfonic acid

3: (i) H₂, Pd-C, (ii) LiAlH₄

4: (i) PBr₃, (ii) /BRN= 4029559/

With sulfuric acid; toluene-4-sulfonic acid; zinc;

Reference yield:

4-Cyclohexyl-2-ethyl-3-hydroxy-butyric acid ethyl ester (22565-36-2) → Thiosulfuric acid S-[2-(4-cyclohexyl-2-ethyl-butylamino)-ethyl] ester (19142-97-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid; toluene-4-sulfonic acid

2: (i) H₂, Pd-C, (ii) LiAlH₄

3: (i) PBr₃, (ii) /BRN= 4029559/

With sulfuric acid; toluene-4-sulfonic acid;

Reference yield:

(E)-4-Cyclohexyl-2-ethyl-but-2-enoic acid ethyl ester (22565-37-3) → Thiosulfuric acid S-[2-(4-cyclohexyl-2-ethyl-butylamino)-ethyl] ester (19142-97-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) H₂, Pd-C, (ii) LiAlH₄

2: (i) PBr₃, (ii) /BRN= 4029559/

upstream raw materials:

thiosulfuric acid S-(2-amino-ethyl) ester; sodium salt

cyclohexylacetaldehyde

(E)-4-Cyclohexyl-2-ethyl-but-2-enoic acid ethyl ester

4-Cyclohexyl-2-ethyl-3-hydroxy-butyric acid ethyl ester