N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

Base Information

Chemical Name:N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide
CAS No.:345625-95-8
Molecular Formula:C₃₁H₅₃NO₅
Molecular Weight:519.766
Hs Code.:

Synonyms:N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

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Chemical Property of N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

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Technology Process of N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

There total 4 articles about N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 111-26-2
hexan-1-amine

: 345625-94-7
4,6-bis-octyloxyisophthalic acid monomethyl ester

: 345625-95-8
N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; Heating;
DOI:10.1021/ja010701b

Reference yield:

: 267897-57-4
dimethyl 4,6-bis(octyloxy)-1,3-benzenedicarboxylate

: 345625-95-8
N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / KOH / dimethylsulfoxide; methanol / 3 h / 130 °C

2: 82 percent / EDC; HOBT / dimethylformamide / Heating

With potassium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja010701b

Reference yield:

: 111-83-1
1-bromo-octane

: 345625-95-8
N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / K₂CO₃ / methanol; dimethylformamide / 48 h / 100 °C

2: 61 percent / KOH / dimethylsulfoxide; methanol / 3 h / 130 °C

3: 82 percent / EDC; 1-hydroxybenzotriazole / dimethylformamide / 5 h / 20 °C

With potassium hydroxide; potassium carbonate; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo010250d