N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

Base Information

Chemical Name:N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide
CAS No.:345625-97-0
Molecular Formula:C₃₄H₅₈N₂O₆
Molecular Weight:590.844
Hs Code.:

Synonyms:N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

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Chemical Property of N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

Chemical Property:

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Technology Process of N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

There total 7 articles about N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 623-33-6
glycine ethyl ester hydrochloride

: 345625-96-9
N-hexyl-2,4-dioctyloxy-5-hydroxycarbonylbenzamide

: 345625-97-0
N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/ja010701b

Reference yield:

: 345625-94-7
4,6-bis-octyloxyisophthalic acid monomethyl ester

: 345625-97-0
N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / EDC; HOBT / dimethylformamide / Heating

2: 94 percent / aq. NaOH / methanol / 0.5 h / Heating

3: 89 percent / EDC; HOBT; Et₃N / dimethylformamide; dimethylsulfoxide / 6 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja010701b

Reference yield:

: 345625-95-8
N-hexyl-2,4-dioctyloxy-5-methoxycarbonylbenzamide

: 345625-97-0
N-ethoxycarbonylmethyl-N'-hexyl-2,4-dioctyloxy-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH / methanol / 0.5 h / Heating

2: 89 percent / EDC; HOBT; Et₃N / dimethylformamide; dimethylsulfoxide / 6 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja010701b