2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

Base Information

Chemical Name:2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate
CAS No.:1448147-60-1
Molecular Formula:C₂₂H₂₆N₂O₇S
Molecular Weight:462.524
Hs Code.:

Synonyms:2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

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Chemical Property of 2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

Chemical Property:

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Technology Process of 2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

There total 6 articles about 2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: potassium 2,3,3-trimethylindole-5-sulfonate

: 1448147-58-7
1-((2-(2-bromoethoxy)ethoxy)methyl)-4-nitrobenzene

: 1448147-60-1
2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: In sulfolane; at 110 ℃; for 16h; Concentration; Sealed tube;

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1448147-60-1
2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: triphenylphosphine; carbon tetrabromide / dichloromethane / 2 h / 0 °C

3.1: sulfolane / 16 h / 110 °C / Sealed tube

With carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; sulfolane; dichloromethane;

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 1448147-60-1
2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 3 h / Reflux

2: potassium hydroxide / methanol; isopropyl alcohol / 0.25 h / Reflux

3: sulfolane / 16 h / 110 °C / Sealed tube

With acetic acid; potassium hydroxide; In sulfolane; methanol; isopropyl alcohol; 1: |Fischer Indole Synthesis;