2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

Base Information

Chemical Name:2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate
CAS No.:1448147-62-3
Molecular Formula:C₄₂H₄₉N₃O₁₂S₂
Molecular Weight:851.996
Hs Code.:

2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

Synonyms:2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

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Chemical Property of 2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

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Technology Process of 2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

There total 8 articles about 2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146368-08-3
1-(5-carboxypentyl)-2,3,3-trimethyl-3H-indolium-5-sulfonate

: 1448147-60-1
2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate

: 58467-94-0
N-((1E,3E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

: 1448147-62-3
2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: 1-(5-carboxypentyl)-2,3,3-trimethyl-3H-indolium-5-sulfonate; N-((1E,3E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride; With acetic anhydride; acetic acid; at 120 ℃; for 2h;

2,3,3-trimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethyl)-3H-indol-1-ium-5-sulfonate; With potassium acetate; at 120 ℃; for 3h; Concentration;

Reference yield:

: potassium 2,3,3-trimethylindole-5-sulfonate

: 1448147-62-3
2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfolane / 16 h / 110 °C / Sealed tube

2.1: acetic anhydride; acetic acid / 2 h / 120 °C

2.2: 3 h / 120 °C

With acetic anhydride; acetic acid; In sulfolane;

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 1448147-62-3
2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(2-(2-((4-nitrobenzyl)oxy)ethoxy)ethtyl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 3 h / Reflux

2.1: potassium hydroxide / methanol; isopropyl alcohol / 0.25 h / Reflux

3.1: sulfolane / 16 h / 110 °C / Sealed tube

4.1: acetic anhydride; acetic acid / 2 h / 120 °C

4.2: 3 h / 120 °C

With acetic anhydride; acetic acid; potassium hydroxide; In sulfolane; methanol; isopropyl alcohol; 1.1: |Fischer Indole Synthesis;