bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ⁵-[1,3,2]oxazaphospholidin-2r-yl)-amine

Base Information

• Chemical Name: bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ⁵-[1,3,2]oxazaphospholidin-2r-yl)-amine
• CAS No.: 97282-19-4
• Molecular Formula: C₁₄H₂₁Cl₂N₂O₂P
• Molecular Weight: 351.213

Synonyms:bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ⁵-[1,3,2]oxazaphospholidin-2r-yl)-amine

Chemical Property of bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ⁵-[1,3,2]oxazaphospholidin-2r-yl)-amine

Chemical Property:

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Technology Process of bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ⁵-[1,3,2]oxazaphospholidin-2r-yl)-amine

There total 2 articles about bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ⁵-[1,3,2]oxazaphospholidin-2r-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pseudoephedrine (90-82-4,7009-81-6,90-83-5,6912-63-6) + N,N-bis(chloro-2-ethyl)amine (334-22-5) → bis-(2-chloro-ethyl)-((2S)-3,4t-dimethyl-2-oxo-5c-phenyl-2λ5-[1,3,2]oxazaphospholidin-2r-yl)-amine (97282-19-4)

Guidance literature:

Multistep reaction; (i) POCl₃, Et₃N, benzene, (ii) /BRN= 605316/;

Reference yield:

→ bis-(2-chloro-ethyl)-(3,4-dimethyl-2-oxo-5-phenyl-2λ5-[1,3,2]oxazaphospholidin-2-yl)-amine (97282-19-4)

Guidance literature:

Aus l-Ephedrin in Ether und Phosphorsaeure-dichlorid-bis-(2-chlorethyl)-amid in sd. Ether (18h);

upstream raw materials:

pseudoephedrine

N,N-bis(chloro-2-ethyl)amine

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