Technology Process of C41H32F3N7
There total 4 articles about C41H32F3N7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H18F3N5;
With
nitrosylsulfuric acid;
In
1-methyl-pyrrolidin-2-one;
at 0 - 5 ℃;
for 1h;
N-(sec-butyl)naphthalen-1-amine;
In
1-methyl-pyrrolidin-2-one; ethanol; water;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 5 °C
2.1: tert.-butylnitrite; hydrofluoroboric acid / tetrahydrofuran / 2 h / 0 - 15 °C
2.2: 1 h / 5 - 15 °C
3.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1 h / 0 - 5 °C
3.2: 1 h / 20 °C
With
hydrogenchloride; tert.-butylnitrite; nitrosylsulfuric acid; hydrofluoroboric acid; sodium nitrite;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butylnitrite; hydrofluoroboric acid / tetrahydrofuran / 2 h / 0 - 15 °C
1.2: 1 h / 5 - 15 °C
2.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1 h / 0 - 5 °C
2.2: 1 h / 20 °C
With
tert.-butylnitrite; nitrosylsulfuric acid; hydrofluoroboric acid;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one;