C₄₂H₅₉IO₇S

Base Information

Chemical Name:C₄₂H₅₉IO₇S
CAS No.:1312705-64-8
Molecular Formula:C₄₂H₅₉IO₇S
Molecular Weight:834.897
Hs Code.:

C<sub>42</sub>H<sub>59</sub>IO<sub>7</sub>S

Synonyms:C₄₂H₅₉IO₇S

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Chemical Property of C₄₂H₅₉IO₇S

Chemical Property:

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Technology Process of C₄₂H₅₉IO₇S

There total 13 articles about C₄₂H₅₉IO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₆₃IO₈S

: 1312705-64-8
C₄₂H₅₉IO₇S

Guidance literature:: With methanol; acetyl chloride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2011.03.149

Reference yield:

: C₃₈H₅₆O₉Si

: 1312705-64-8
C₄₂H₅₉IO₇S

Guidance literature:: Multi-step reaction with 11 steps

1.1: dimethylsulfide; boron trifluoride diethyl etherate / 1 h / -20 °C

2.1: dmap; triethylamine / dichloromethane / 16 h / 35 °C

3.1: potassium carbonate / methanol / 3 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 35 °C

5.1: n-butyllithium; diethylaluminium chloride / toluene / 0.33 h / 0 °C

6.1: potassium carbonate / methanol / 2 h / 20 °C

7.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1 h / 20 °C

7.2: 18 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane / 2 h / 30 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C

10.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C

11.1: methanol; acetyl chloride / tetrahydrofuran / 1 h / 0 °C

With methanol; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dimethylsulfide; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; diethylaluminium chloride; potassium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; acetyl chloride; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; toluene; 7.1: Sonogashira coupling / 8.1: Dess-Martin oxidation / 10.1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2011.03.149

Reference yield:

: C₃₈H₆₀O₈S

: 1312705-64-8
C₄₂H₅₉IO₇S

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C

2: methanol; acetyl chloride / tetrahydrofuran / 1 h / 0 °C

With methanol; di-isopropyl azodicarboxylate; acetyl chloride; triphenylphosphine; In tetrahydrofuran; 1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2011.03.149