Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Base Information

Chemical Name:Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol
CAS No.:159217-52-4
Molecular Formula:C₇₉H₁₀₄O₃
Molecular Weight:1101.69
Hs Code.:

Synonyms:Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Suppliers and Price of Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

There total 4 articles about Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 26537-19-9
methyl 4-tert-butylbenzoate

: 151160-13-3
<(3-Bromo-4,6-di-isopropylphenyl)bis(4-tert-butylphenyl)methoxy>methane

: 159217-52-4
Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Guidance literature:: With tert.-butyl lithium; In diethyl ether; pentane; 1.) -78 deg C, 60 min, 2.) -78 deg C to r.t., overnight;
DOI:10.1021/jo00102a041

Reference yield:

: 15796-82-4
4,4'-di-tert-butylbenzophenone

: 159217-52-4
Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / n-BuLi / diethyl ether; hexane / 1.) -10 deg C, 35 min, 2.) -10 deg C to r.t., overnight

2: 92 percent / NaH / tetrahydrofuran / 0 deg C to r.t.

3: 90 percent / t-BuLi / pentane; diethyl ether / 1.) -78 deg C, 60 min, 2.) -78 deg C to r.t., overnight

With n-butyllithium; tert.-butyl lithium; sodium hydride; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1021/jo00102a041

Reference yield:

: 40734-61-0
4,6-dibromo-1,3-diisopropylbenzene

: 159217-52-4
Bis-{5-[bis-(4-tert-butyl-phenyl)-methoxy-methyl]-2,4-diisopropyl-phenyl}-(4-tert-butyl-phenyl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / n-BuLi / diethyl ether; hexane / 1.) -10 deg C, 35 min, 2.) -10 deg C to r.t., overnight

2: 92 percent / NaH / tetrahydrofuran / 0 deg C to r.t.

3: 90 percent / t-BuLi / pentane; diethyl ether / 1.) -78 deg C, 60 min, 2.) -78 deg C to r.t., overnight

With n-butyllithium; tert.-butyl lithium; sodium hydride; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1021/jo00102a041