1-ethyl-3,5,7-trimethyladamantane

Base Information

• Chemical Name: 1-ethyl-3,5,7-trimethyladamantane
• CAS No.: 2109-06-0
• Molecular Formula: C₁₅H₂₆
• Molecular Weight: 206.371

Synonyms:1-ethyl-3,5,7-trimethyladamantane

Chemical Property of 1-ethyl-3,5,7-trimethyladamantane

Chemical Property:

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Technology Process of 1-ethyl-3,5,7-trimethyladamantane

There total 7 articles about 1-ethyl-3,5,7-trimethyladamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

tetramethylsilane (75-76-3) + 1-ethyladamantane (770-69-4) → 1-ethyl-3,5,7-trimethyladamantane (2109-06-0)

Guidance literature:

With aluminum (III) chloride; In dichloromethane; at 20 ℃; for 120h; Sealed tube;

DOI:10.1002/ejoc.202101004

Reference yield: 6.47%

methyl cyclohexane (82166-21-0) → 1-ethyl-3-methyladamantane (1687-34-9) + 1,3-Dimethyl-5-ethyladamantane (1687-35-0) + 1-ethyl-3,5,7-trimethyladamantane (2109-06-0)

Guidance literature:

With aluminium trichloride; tertiary butyl chloride; at 160 ℃; for 15h; Product distribution;

Reference yield: 3.15%

ethyl-cyclohexane (1678-91-7) → 1-ethyl-3-methyladamantane (1687-34-9) + 1,3-Dimethyl-5-ethyladamantane (1687-35-0) + 1-ethyl-3,5,7-trimethyladamantane (2109-06-0)

Guidance literature:

With aluminium trichloride; tertiary butyl chloride; at 160 ℃; for 15h; Product distribution;

upstream raw materials:

tetramethylsilane

adamantane

ethyl-cyclohexane

(1-methylethyl)-cyclohexane

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