(S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate

Base Information

Chemical Name:(S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate
CAS No.:1147106-84-0
Molecular Formula:C₃₆H₄₂BrNO₄
Molecular Weight:632.638
Hs Code.:

Synonyms:(S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate

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Technology Process of (S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate

There total 1 articles about (S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 2111-53-7,57030-77-0
(S)-(-)-citronellic acid

: 1147106-71-5
(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

: 1147106-84-0
(S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate

Guidance literature:: (2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate; With diphenylphosphinopolystyrene; In tetrahydrofuran; at 20 ℃; for 12h;

With triethylamine; In tetrahydrofuran; for 12h; Reflux;

(S)-(-)-citronellic acid; With oxygen; In toluene; at 60 ℃; for 0.5h; Molecular sieve;

Reference yield:

: 1147106-84-0
(S)-((S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl) 3,7-dimethyloct-6-enoate

: 1147106-85-1
C₃₂H₃₄BrNO₄

: C₃₂H₃₄BrNO₄

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In toluene; at 60 ℃; for 11h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;