(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

Base Information

Chemical Name:(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate
CAS No.:1147106-71-5
Molecular Formula:C₂₆H₂₆BrN₃O₃
Molecular Weight:508.415
Hs Code.:

Synonyms:(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

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Technology Process of (2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

There total 1 articles about (2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1147106-44-2
1-(4-bromophenyl)hept-6-en-1-yn-3-yl but-2-ynoate

: 439694-28-7
(S)-2-azido-3-phenyl-propan-1-ol

: 1147106-71-5
(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

Guidance literature:: With silver hexafluoroantimonate; (tri-tert-butylphosphane)gold(I) chloride; In dichloromethane; at 20 ℃; regioselective reaction;

Reference yield: 70.0%

: 1147106-71-5
(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

: 1147106-73-7
((3S,5S)-3-benzyl-5-(but-3-enyl)-7-methyl-3,5-dihydro-2H-oxazolo[3,2-α]pyridin-6-yl)(4-bromophenyl)methanoate

Guidance literature:: With triethylamine; triphenylphosphine; In tetrahydrofuran; for 24h; Reflux;

Reference yield: 65.0%

: 591-80-0
pent-4-enoic acid

: 1147106-71-5
(2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate

: 1147106-74-8
(S)-2-(5-(4-bromobenzoyl)-6-(but-3-enyl)-4-methyl-2-oxopyridin-1(2H)-yl)-3-phenylpropyl pent-4-enoate

Guidance literature:: (2Z,4E)-((S)-2-azido-3-phenylpropyl) 4-(4-bromobenzoyl)-3-methylnona-2,4,8-trienoate; With diphenylphosphinopolystyrene; In tetrahydrofuran; at 20 ℃; for 12h;

With triethylamine; In tetrahydrofuran; for 12h; Reflux;

pent-4-enoic acid; With oxygen; In toluene; at 60 ℃; for 0.5h; Molecular sieve;