11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

Base Information

Chemical Name:11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate
CAS No.:901128-79-8
Molecular Formula:C₇H₈O₃S*C₂₈H₂₇N₇O
Molecular Weight:649.773
Hs Code.:

Synonyms:11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

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Chemical Property of 11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

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Technology Process of 11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

There total 3 articles about 11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.3%

: 856691-93-5
CEP-11981

: 104-15-4
toluene-4-sulfonic acid

: 901128-79-8
11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

Guidance literature:: In dichloromethane; at 10 ℃; for 1h; Industry scale;

Reference yield:

: 855260-38-7
11-(2-methylpropyl)-12,13-dihydro-2-methyl-8-amino-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one

: 901128-79-8
11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / butan-1-ol / 20 h / 117 °C / Industry scale

1.2: 0.25 h / 75 °C / Industry scale

2.1: Isopropyl acetate / 10 - 70 °C / Industry scale

3.1: dichloromethane / 1 h / 10 °C / Industry scale

With triethylamine; In dichloromethane; Isopropyl acetate; butan-1-ol;

Reference yield:

: 2C₂H₄O₂*C₂₈H₂₇N₇O

: 901128-79-8
11-isobutyl-2-methyl-8-(2-pyrimidinylamino)-2,5,6,11,12,13-hexahydro-4H-indazolo[5,4-a]pyrrolo[3,4-c]carbazol-4-one para-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: Isopropyl acetate / 10 - 70 °C / Industry scale

2: dichloromethane / 1 h / 10 °C / Industry scale

In dichloromethane; Isopropyl acetate;