methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

Base Information

Chemical Name:methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate
CAS No.:1207956-21-5
Molecular Formula:C₁₉H₁₉F₃N₂O₄
Molecular Weight:396.366
Hs Code.:

Synonyms:methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

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Chemical Property of methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

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Technology Process of methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

There total 4 articles about methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1160492-16-9
methyl N-(5-acetyl-2-methylphenoxy)carbamate

: 215599-92-1
O-(2-trifluoromethylbenzyl)hydroxylamine hydrochloride

: 1207956-21-5
methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

Guidance literature:: In methanol; for 2h; Reflux;

Reference yield:

: 51436-99-8
2-fluoro-4-bromotoluene

: 1207956-21-5
methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / 1,5-dimethyl-2-imidazolidone / 1 h / 110 °C

2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C

2.3: -78 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: potassium tert-butylate / methanol / 1 h / 20 °C

4.2: 0.17 h / Cooling with ice

4.3: 1 h

5.1: methanol / 2 h / Reflux

With n-butyllithium; potassium tert-butylate; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,5-dimethyl-2-imidazolidone; dichloromethane;

Reference yield:

: 1207956-22-6
4-bromo-2-(4-methoxybenzyloxy)-1-methylbenzene

: 1207956-21-5
methyl N-{2-methyl-5-[1-(2-trifluoromethylbenzyloxyimino)ethyl]phenoxy}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 °C

1.3: -78 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: potassium tert-butylate / methanol / 1 h / 20 °C

3.2: 0.17 h / Cooling with ice

3.3: 1 h

4.1: methanol / 2 h / Reflux

With n-butyllithium; potassium tert-butylate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;