1-benzyl-1,10-phenanthrolin-1-ium bromide

Base Information

Chemical Name:1-benzyl-1,10-phenanthrolin-1-ium bromide
CAS No.:368887-68-7
Molecular Formula:Br*C₁₉H₁₅N₂
Molecular Weight:351.245
Hs Code.:

Synonyms:1-benzyl-1,10-phenanthrolin-1-ium bromide

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Chemical Property of 1-benzyl-1,10-phenanthrolin-1-ium bromide

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Technology Process of 1-benzyl-1,10-phenanthrolin-1-ium bromide

There total 1 articles about 1-benzyl-1,10-phenanthrolin-1-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 66-71-7
1,10-Phenanthroline

: 100-39-0
benzyl bromide

: 368887-68-7
1-benzyl-1,10-phenanthrolin-1-ium bromide

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; for 5h; Reflux;

Reference yield: 96.0%

: [Ir(cod)₂]SbF₆

: 368887-68-7
1-benzyl-1,10-phenanthrolin-1-ium bromide

: (IrHBr(C₈H₁₂)(NC₁₂H₇NCH₂C₆H₅))⁽¹⁺⁾*SbF₆^(1-)=(IrHBr(C₈H₁₂)(NC₁₂H₇NCH₂C₆H₅))SbF₆

Guidance literature:: In dichloromethane; under N2 atm. to soln. Ir complex in CH2Cl2 pyridinium salt was added and stirred at room temp. for 12 h; soln. was concd., Et2O was added, ppt. was filtered and dried, recrystn.from CH2Cl2-Et2O; elem. anal.;
DOI:10.1021/om800756c