4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

Base Information

Chemical Name:4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid
CAS No.:1294397-87-7
Molecular Formula:C₂₇H₄₄N₂O₄
Molecular Weight:460.657
Hs Code.:

Synonyms:4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

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Chemical Property of 4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

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Technology Process of 4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

There total 4 articles about 4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1294397-86-6
methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

: 1294397-87-7
4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c0cc05474g

Reference yield:

: 1269504-41-7
4-(1-bromo-2-methylpropyl)-benzoic acid

: 1294397-87-7
4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 5 h / 20 °C / Inert atmosphere

2: copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 17 h / 55 °C / Inert atmosphere

3: sodium hydroxide / methanol / 2 h / 20 °C / Inert atmosphere

With thionyl chloride; copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine; sodium hydroxide; In methanol; benzene;
DOI:10.1039/c0cc05474g

Reference yield:

: 947769-95-1
4-(1-bromo-2-methylpropyl)-benzaldehyde

: 1294397-87-7
4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: Jones reagent / acetone / 1 h / 0 °C / Inert atmosphere

2: thionyl chloride / 5 h / 20 °C / Inert atmosphere

3: copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 17 h / 55 °C / Inert atmosphere

4: sodium hydroxide / methanol / 2 h / 20 °C / Inert atmosphere

With Jones reagent; thionyl chloride; copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine; sodium hydroxide; In methanol; acetone; benzene;
DOI:10.1039/c0cc05474g