methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

Base Information

Chemical Name:methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate
CAS No.:1294397-86-6
Molecular Formula:C₂₈H₄₆N₂O₄
Molecular Weight:474.684
Hs Code.:

Synonyms:methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

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Chemical Property of methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

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Technology Process of methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

There total 3 articles about methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1294397-83-3
methyl-4-(1-bromo-2-methylpropyl)-benzoate

: 4-tert-butyl-2,2,6,6-tetraethyl-3-oxo-piperazin-1-oxyl radical

: 1294397-86-6
methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine; In benzene; at 55 ℃; for 17h; Inert atmosphere;
DOI:10.1039/c0cc05474g

Reference yield:

: 947769-95-1
4-(1-bromo-2-methylpropyl)-benzaldehyde

: 1294397-86-6
methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent / acetone / 1 h / 0 °C / Inert atmosphere

2: thionyl chloride / 5 h / 20 °C / Inert atmosphere

3: copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 17 h / 55 °C / Inert atmosphere

With Jones reagent; thionyl chloride; copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine; In acetone; benzene;
DOI:10.1039/c0cc05474g

Reference yield:

: 1269504-41-7
4-(1-bromo-2-methylpropyl)-benzoic acid

: 1294397-86-6
methyl-4-(1-[{4-(tert-butyl)-2,2,6,6-tetraethyl-3-oxopiperazin-1-yl}oxy]-2-methylpropyl)-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 5 h / 20 °C / Inert atmosphere

2: copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 17 h / 55 °C / Inert atmosphere

With thionyl chloride; copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine; In benzene;
DOI:10.1039/c0cc05474g