(Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾2ClO₄^(1-)H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O

Base Information

Chemical Name:(Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O
CAS No.:78891-47-1
Molecular Formula:C₇H₂₃CoN₆O₂S*2ClO₄*H₂O
Molecular Weight:531.274
Hs Code.:

(Co(NH<sub>3</sub>)5(NHSO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>))<sup>(2+)</sup>*2ClO<sub>4</sub><sup>(1-)</sup>*H<sub>2</sub>O=(Co(NH<sub>3</sub>)5(NHSO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>))(ClO<sub>4</sub>)2*H<sub>2</sub>O

Synonyms:(Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O

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Chemical Property of (Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O

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Technology Process of (Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O

There total 2 articles about (Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115245-01-7
trifluoromethanesulfonatopentaamminecobalt(III) trifluoromethanesulfonate

: 70-55-3
toluene-4-sulfonamide

: 78891-47-1
Co(NH₃)5(NHSO₂C₆H₄CH₃)⁽²⁺⁾*2ClO₄^(1-)=Co(NH₃)5(NHSO₂C₆H₄CH₃)(ClO₄)2

Guidance literature:: With 2,6-dimethylpyridine; sodium perchlorate; In sulfolane; methanol; Co complex and 2,6-dimethylpyridine adding to sulfonamide in sulfolane,after 4 h at 40°C filtering into 2-butanol and Et2O, solvent decanting off, residue drying in vacuo, dissolving in MeOH, conc. NaClO4 inMeOH adding, cooling, ppt. sepg. off; purified by recrystn. from MeOH; identified by elem. anal., IR, UV and NMR spectra;
DOI:10.1021/ic00135a074

Reference yield:

: 13820-81-0
aquapentaamminecobalt(III) perchlorate

: sodium perchlorate

: 70-55-3
toluene-4-sulfonamide

: 78891-47-1
(Co(NH₃)5(NHSO₂C₆H₄CH₃))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄CH₃))(ClO₄)2*H₂O

Guidance literature:: With 2,6-dimethylpyridine; In N,N-dimethyl acetamide; soln. (Co(NH3)5(H2O))(ClO4)3 in dry dimethylacetamide mixed with soln. p-toluenesulfonamide and 2,6-lutidine in dimethylacetamide, soln. heatedfor 6 h on steam bath, cooled, filtered and dropped into 50:50 mixt. ether and 2-butanol; product purified by ion-exchange chromy. on Baker CGC-271 in Na(1+) form (eluted with NaClO4 soln., product at the top column separated, washedwith water, acetic acid), NaOH and NaClO4 added, complex recrystd. fromwater, washed with ether; elem. anal.;
DOI:10.1021/ic00133a003