4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

Base Information

Chemical Name:4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine
CAS No.:1432670-66-0
Molecular Formula:C₂₈H₂₄N₃P
Molecular Weight:433.492
Hs Code.:

Synonyms:4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

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Chemical Property of 4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

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Technology Process of 4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

There total 4 articles about 4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1432670-65-9
N-(2-iodophenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

: 829-85-6
diphenylphosphane

: 1432670-66-0
4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; for 15h; Reagent/catalyst; Solvent; Time; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1021/om400151e

Reference yield:

: 615-42-9
1,2-Diiodobenzene

: 1432670-66-0
4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; caesium carbonate / 1,4-dioxane / 15 h / Inert atmosphere; Schlenk technique; Reflux

2: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; triethylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 15 h / Inert atmosphere; Schlenk technique; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane;
DOI:10.1021/om400151e

Reference yield:

: N-(2-amino-5-methylphenyl)-1H-pyrazole

: 1432670-66-0
4-methyl-N-(2-(diphenylphosphino)phenyl)-2-(1H-pyrazol-1-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; caesium carbonate / 1,4-dioxane / 15 h / Inert atmosphere; Schlenk technique; Reflux

2: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; triethylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 15 h / Inert atmosphere; Schlenk technique; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane;
DOI:10.1021/om400151e