C₁₀H₁₇N₂OPS

Base Information

• Chemical Name: C₁₀H₁₇N₂OPS
• CAS No.: 160194-60-5
• Molecular Formula: C₁₀H₁₇N₂OPS
• Molecular Weight: 244.298
• Mol file: 160194-60-5.mol

Synonyms:C₁₀H₁₇N₂OPS

Chemical Property of C₁₀H₁₇N₂OPS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₇N₂OPS

There total 3 articles about C₁₀H₁₇N₂OPS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.8%

N-(2-Mercaptoethyl)-P-phenyl-P-(2-phthalimidoethyl)phosphinsaeureamid (160194-57-0) → C10H17N2OPS (160194-60-5)

Guidance literature:

With hydrazine hydrate; In ethanol; for 3h; Heating;

DOI:10.1002/hlca.19940770612

Reference yield:

C16H13ClNO3P → C10H17N2OPS (160194-60-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 34.8 percent / Et₃N / CHCl₃ / 4 h / Heating

2: 72.8 percent / 100percent hydrazine hydrate / ethanol / 3 h / Heating

With hydrazine hydrate; triethylamine; In ethanol; chloroform;

DOI:10.1002/hlca.19940770612

Reference yield:

Phenyl(2-phthalimidoethyl)phosphinsaeure-ethylester (160194-54-7) → C10H17N2OPS (160194-60-5)

Guidance literature:

Multi-step reaction with 3 steps

1: PCl₅ / toluene / 12 h / Heating

2: 34.8 percent / Et₃N / CHCl₃ / 4 h / Heating

3: 72.8 percent / 100percent hydrazine hydrate / ethanol / 3 h / Heating

With phosphorus pentachloride; hydrazine hydrate; triethylamine; In ethanol; chloroform; toluene;

DOI:10.1002/hlca.19940770612

upstream raw materials:

N-(2-Mercaptoethyl)-P-phenyl-P-(2-phthalimidoethyl)phosphinsaeureamid

Phenyl(2-phthalimidoethyl)phosphinsaeure-ethylester