bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

Base Information

Chemical Name:bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine
CAS No.:1257423-30-5
Molecular Formula:C₅₈H₇₈B₂N₂O₄
Molecular Weight:888.89
Hs Code.:

Synonyms:bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

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Chemical Property of bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

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Technology Process of bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

There total 4 articles about bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1257423-29-2
bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-bromophenyl)-1,4-phenylenediamine

: 1257423-30-5
bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

Guidance literature:: bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-bromophenyl)-1,4-phenylenediamine; With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1039/c0jm01641a

Reference yield:

: 74-31-7,943443-44-5
N,N'-diphenyl-1,4-phenylenediamine

: 1257423-30-5
bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate / toluene / 48 h / 120 °C / Inert atmosphere

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

3.2: -78 - 20 °C

With N-Bromosuccinimide; n-butyllithium; tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c0jm01641a

Reference yield:

: 1257423-28-1
bis-N,N'-(4-octylphenyl)-bis-N,N'-phenyl-1,4-phenylenediamine

: 1257423-30-5
bis-N,N'-(4-octylphenyl)-bis-N,N'-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)phenyl)-1,4-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

2.2: -78 - 20 °C

With N-Bromosuccinimide; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0jm01641a