potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

Base Information

Chemical Name:potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate
CAS No.:960240-12-4
Molecular Formula:C₂₆H₂₁Cl₂N₂O₃*K
Molecular Weight:519.469
Hs Code.:

Synonyms:potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

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Chemical Property of potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

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Technology Process of potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

There total 6 articles about potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1050656-19-3
methyl 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

: 960240-12-4
potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

Guidance literature:: With potassium hydroxide; ethanol; water; at 80 ℃; for 2h;

Reference yield:

: 1129-35-7
4-cyanobenzoic acid methyl ester

: 960240-12-4
potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: titanium(IV) isopropylate / tetrahydrofuran; toluene / 2.5 h / -25 °C

1.2: 1.33 h / -25 °C

1.3: -25 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 2 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane

4.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 70 °C

5.1: potassium hydroxide; ethanol; water / 2 h / 80 °C

With potassium hydroxide; ethanol; water; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; titanium(IV) isopropylate; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: 1006037-03-1
4-(1-aminocyclopropyl)-benzoic acid methyl ester

: 960240-12-4
potassium 4-[1-({[1-(3,4-dichloro-benzyl)-2,3-dihydro-1H-indol-7-yl]carbonyl}amino)cyclopropyl]-benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 2 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane

3: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 70 °C

4: potassium hydroxide; ethanol; water / 2 h / 80 °C

With potassium hydroxide; ethanol; water; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In dichloromethane; acetonitrile;