benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

Base Information

Chemical Name:benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate
CAS No.:1052213-43-0
Molecular Formula:C₃₁H₃₂N₂O₇
Molecular Weight:544.604
Hs Code.:

Synonyms:benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

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Chemical Property of benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

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Technology Process of benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

There total 2 articles about benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 132836-66-9
(S)-3-acetyl-4-benzyloxazolidin-2-one

: 439589-23-8
(S)-2-(((benzyloxy)carbonyl)(4-methoxybenzyl)amino)propanoic acid

: 1052213-43-0
benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

Guidance literature:: (S)-2-(((benzyloxy)carbonyl)(4-methoxybenzyl)amino)propanoic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; Inert atmosphere;

(S)-3-acetyl-4-benzyloxazolidin-2-one; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo801993k

Reference yield:

: C₂₂H₂₃N₃O₄

: 132836-66-9
(S)-3-acetyl-4-benzyloxazolidin-2-one

: 1052213-43-0
benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

Guidance literature:: (S)-3-acetyl-4-benzyloxazolidin-2-one; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₂₂H₂₃N₃O₄; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo801258h

Reference yield: 71.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-11-6
diiodomethane

: 1052213-43-0
benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

: 1052213-45-2
benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

Guidance literature:: diiodomethane; With diethylzinc; In hexane; dichloromethane; at 0 ℃; Inert atmosphere;

formaldehyd; benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate; In hexane; dichloromethane; for 1h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo801993k