benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

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Chemical Name:benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate
CAS No.:1052213-45-2
Molecular Formula:C₃₃H₃₆N₂O₈
Molecular Weight:588.657
Hs Code.:

Synonyms:benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

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Chemical Property of benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

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Technology Process of benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

There total 2 articles about benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-11-6
diiodomethane

: 1052213-43-0
benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

: 1052213-45-2
benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

Guidance literature:: diiodomethane; With diethylzinc; In hexane; dichloromethane; at 0 ℃; Inert atmosphere;

formaldehyd; benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate; In hexane; dichloromethane; for 1h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo801993k

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-11-6
diiodomethane

: 1052213-43-0
benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate

: 1052213-45-2
benzyl [(2R,5R)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-(hydroxymethyl)-3,6-dioxohexan-2-yl](4-methoxybenzyl)carbamate

: C₃₄H₃₈N₂O₉

Guidance literature:: formaldehyd; diiodomethane; benzyl [(R)-5-((S)-4-benzyl-2-oxooxazolidin-3-yl)-3,5-dioxopentan-2-yl](4-methoxybenzyl)carbamate; With diethylzinc; In hexane; dichloromethane; for 1h; Inert atmosphere;

With water; ammonium chloride; In hexane; dichloromethane; Inert atmosphere;
DOI:10.1021/jo801258h