((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

Base Information

Chemical Name:((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide
CAS No.:1443050-82-5
Molecular Formula:C₃₃H₃₄Br₂N₂Ni
Molecular Weight:677.144
Hs Code.:

Synonyms:((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

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Chemical Property of ((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

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Technology Process of ((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

There total 3 articles about ((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 1443050-76-7
1-(2,6-diisopropylphenylimino)-2-(2,4,6-trimethylphenylimino)acenaphthylenylidene

: 1443050-82-5
((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

Guidance literature:: In dichloromethane; at 20 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1080/00958972.2015.1057130

Reference yield:

: 82-86-0
acenaphthene quinone

: 1443050-82-5
((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / ethanol / 16 h / 60 °C

2: toluene-4-sulfonic acid / tetrahydrofuran / 17 h / Reflux; Molecular sieve

3: dichloromethane / 24 h / 20 °C / Schlenk technique; Inert atmosphere

With formic acid; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1080/00958972.2015.1057130

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1443050-82-5
((2,6-diisopropylphenyl)imino)((2,4,6-trimethylphenyl)imino)acenaphthenenickel(II) dibromide

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / ethanol / 16 h / 60 °C

2: toluene-4-sulfonic acid / tetrahydrofuran / 17 h / Reflux; Molecular sieve

3: dichloromethane / 24 h / 20 °C / Schlenk technique; Inert atmosphere

With formic acid; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1080/00958972.2015.1057130