[(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane

Base Information

• Chemical Name: [(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane
• CAS No.: 1010821-34-7
• Molecular Formula: C₂₉H₃₉BrO₇Si
• Molecular Weight: 607.614

Synonyms:[(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane

Chemical Property of [(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane

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Technology Process of [(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane

There total 1 articles about [(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[(2R,4R,1''R,2''S,5R)-2-phenyl-4-(1'',2''-isopropylidenedioxy-3''-tert-butyldimethylsilyloxypropyl)-5-(3',4'-methylenedioxy)phenyl]-1,3-dioxane (1004760-73-9) → [(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane (1010821-34-7)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In benzene; at 60 ℃; for 1h;

DOI:10.1021/np0705460

Reference yield: 85.0%

[(2R,3R,4S,5S)-1-bromo-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane (1010821-34-7) → [(2R,3R,4S,5S)-1-azido-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane (1010821-35-8)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 5h;

DOI:10.1021/np0705460

upstream raw materials:

[(2R,4R,1''R,2''S,5R)-2-phenyl-4-(1'',2''-isopropylidenedioxy-3''-tert-butyldimethylsilyloxypropyl)-5-(3',4'-methylenedioxy)phenyl]-1,3-dioxane

Downstream raw materials:

[(2R,3R,4S,5S)-1-azido-2-(3',4'-methylenedioxy)phenyl-3-(O)-benzoyl-4,5-isopropylidenedioxy-6-tert-butyldimethylsilyloxy]hexane

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