methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate

Base Information

• Chemical Name: methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate
• CAS No.: 212513-10-5
• Molecular Formula: C₃₀H₃₂O₆S
• Molecular Weight: 520.646

Synonyms:methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate

Chemical Property of methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate

Chemical Property:

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Technology Process of methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate

There total 1 articles about methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl (2R)-2-methoxy-3-(triphenylmethoxy)propanoate (16814-88-3) + 3-(tert-butylthio)-3-oxopropanoic acid (83610-97-3) → methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate (212513-10-5)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1021/jm0100741

Reference yield:

octanol (111-87-5) + methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate (212513-10-5) → Malonic acid (R)-1-methoxycarbonyl-2-trityloxy-ethyl ester octyl ester (212513-27-4)

Guidance literature:

With silver trifluoroacetate; In tetrahydrofuran; at 23 ℃;

DOI:10.1021/jm0100741

Reference yield:

Linoleyl alcohol (506-43-4) + methyl (R)-2-[((tert-butylthio)carbonyl)acetyloxy]-3-triphenylmethyloxypropionate (212513-10-5) → Malonic acid (R)-1-methoxycarbonyl-2-trityloxy-ethyl ester (9Z,12Z)-octadeca-9,12-dienyl ester (212513-19-4)

Guidance literature:

With silver trifluoroacetate; In tetrahydrofuran; at 23 ℃;

DOI:10.1021/jm0100741

upstream raw materials:

methyl (2R)-2-methoxy-3-(triphenylmethoxy)propanoate

3-(tert-butylthio)-3-oxopropanoic acid

Downstream raw materials:

Malonic acid (R)-1-methoxycarbonyl-2-trityloxy-ethyl ester octyl ester

Malonic acid (R)-1-methoxycarbonyl-2-trityloxy-ethyl ester (9Z,12Z)-octadeca-9,12-dienyl ester

Malonic acid decyl ester (R)-1-methoxycarbonyl-2-trityloxy-ethyl ester

Malonic acid dodecyl ester (R)-1-methoxycarbonyl-2-trityloxy-ethyl ester

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