(+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

Base Information

Chemical Name:(+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit
CAS No.:26277-37-2
Molecular Formula:C₄₈H₄₉O₉P
Molecular Weight:800.885
Hs Code.:

Synonyms:(+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

Suppliers and Price of (+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

Chemical Property:

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Technology Process of (+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

There total 7 articles about (+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-39-0
benzyl bromide

: Phosphoric acid mono-((1R,2S,3S,4R,5S,6R)-2,3,4,5-tetrakis-benzyloxy-6-phosphonooxy-cyclohexyl) ester

: 115432-19-4,141040-38-2
(+/-)-1,2,3,4-Tetra-O-benzyl-myo-inositol 5,6-bis(dinbenzyl phosphate)

: 26277-37-2
(+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

Guidance literature:: With 3 A molecular sieve; silver carbonate; In toluene; Heating;
DOI:10.1016/0008-6215(96)00084-5

Reference yield: 88.0%

: 18997-19-8
Chloromethyl pivalate

: Phosphoric acid mono-((1R,2S,3S,4R,5S,6R)-2,3,4,5-tetrakis-benzyloxy-6-phosphonooxy-cyclohexyl) ester

: 26277-37-2
(+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

: 2,2-Dimethyl-propionic acid (2,2-dimethyl-propionyloxymethoxy)-{(1R,2S,3R,4S,5S,6R)-2,3,4,5-tetrakis-benzyloxy-6-[bis-(2,2-dimethyl-propionyloxymethoxy)-phosphoryloxy]-cyclohexyloxy}-phosphoryloxymethyl ester

Guidance literature:: With 3 A molecular sieve; silver carbonate; In toluene; Heating;
DOI:10.1016/0008-6215(96)00084-5

Reference yield:

: 6195-45-5,13264-84-1,22132-86-1,25018-91-1,26277-05-4,28366-79-2,30694-52-1
DL-2,3,4,5,6-penta-O-benzyl-myo-inositol

: 26277-37-2
(+/-)-2,3,4,5,6-O-Pentabenzyl-1-O-hydroxy-benzyloxyphosphoryl-myo-inosit

Guidance literature:: Multi-step reaction with 4 steps

1: tetrazole / acetonitrile; CH₂Cl₂ / 1 h / 20 °C

2: 2 g / m-chloroperbenzoic acid / CH₂Cl₂ / 2 h

3: 1) NaOH, 2) Amberlite IR-120(H⁺) / 1) MeOH, H₂O, 60 deg C, 1 h, 2) MeOH, H₂O

4: Ag₂CO₃, 3 Angstroem molecular sieves / toluene / 3 h / Heating

With 1H-tetrazole; sodium hydroxide; 3 A molecular sieve; Amberlite IR-120(H⁺); 3-chloro-benzenecarboperoxoic acid; silver carbonate; In dichloromethane; toluene; acetonitrile;
DOI:10.1016/0008-6215(96)00084-5