12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone

Base Information

Chemical Name:12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone
CAS No.:1356230-07-3
Molecular Formula:C₂₅H₂₃N₃OS
Molecular Weight:413.543
Hs Code.:

Synonyms:12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone

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Chemical Property of 12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone

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Technology Process of 12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone

There total 2 articles about 12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1173694-48-8
12-(4-methylphenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one

: 79-19-6
thiosemicarbazide

: 1356230-07-3
12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone

Guidance literature:: With acetic acid; In methanol; chloroform; for 24h; Reflux;
DOI:10.1016/j.molstruc.2011.11.003

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 504-02-9
1,3-cylohexanedione

: 135-19-3
β-naphthol

: 1356230-07-3
12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one thiosemicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / ethanol / 3 h / Reflux

2: acetic acid / methanol; chloroform / 24 h / Reflux

With boron trifluoride diethyl etherate; acetic acid; In methanol; ethanol; chloroform;
DOI:10.1016/j.molstruc.2011.11.003