1-Acetyl-2-picolinoylhydrazine

Base Information

Chemical Name:1-Acetyl-2-picolinoylhydrazine
CAS No.:17433-31-7
Molecular Formula:C8H11N3O2
Molecular Weight:179.20
Hs Code.:2933399090
NSC Number:68626
UN Number:2811
UNII:186TH42ZNH
DSSTox Substance ID:DTXSID2024408
Nikkaji Number:J54.014E
Wikidata:Q81983886
NCI Thesaurus Code:C1007
ChEMBL ID:CHEMBL475125
Mol file:17433-31-7.mol

Synonyms:azapicyl;NSC 68626;NSC-68626

Suppliers and Price of 1-Acetyl-2-picolinoylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-ACETYL-2-PICOLINOYLHYDRAZINE 95.00%
5MG
$ 503.61

Total 5 raw suppliers

Chemical Property of 1-Acetyl-2-picolinoylhydrazine

Chemical Property:

Vapor Pressure:1.37E-08mmHg at 25°C
Refractive Index:1.7400 (estimate)
Boiling Point:458.4°C at 760 mmHg
Flash Point:231.1°C
PSA：71.09000
Density:1.231g/cm³
LogP:0.64430
XLogP3:-0.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:179.069476538
Heavy Atom Count:13
Complexity:206
Transport DOT Label:Poison

Purity/Quality:

99% ^*data from raw suppliers

1-ACETYL-2-PICOLINOYLHYDRAZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NNC(=O)C1=CC=CC=N1

Technology Process of 1-Acetyl-2-picolinoylhydrazine

There total 1 articles about 1-Acetyl-2-picolinoylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17433-31-7
N-acetyl-N'-(2-pyridoyl)hydrazine

Guidance literature:: Aus entspr. Hydrazid + Eg./Ac2O;

Reference yield: 54.6%

: 4,4'-dibromophenylphosphazoanilide

: 17433-31-7
N-acetyl-N'-(2-pyridoyl)hydrazine

: 1234570-30-9
3-methyl-4-(p-bromophenyl)-5-(2-pyridyl)-1,2,4-triazole

Guidance literature:: In 1,2-dichloro-benzene; at 180 - 190 ℃; for 3h;
DOI:10.1007/s11224-009-9569-y

Reference yield: 50.0%

: 5679-59-4
diphenylphosphazoanilide

: 17433-31-7
N-acetyl-N'-(2-pyridoyl)hydrazine

: 14664-84-7
3-methyl-4-phenyl-5-(2-pyridyl)-1,2,4-triazole

Guidance literature:: diphenylphosphazoanilide; N-acetyl-N'-(2-pyridoyl)hydrazine; With N,N-dimethyl-aniline; at 189.84 - 199.84 ℃; for 3h;

With hydrogenchloride; water; for 1h; Reflux;

With potassium carbonate; In water; pH=8 - 9;
DOI:10.1007/s10870-009-9583-3