{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Base Information

Chemical Name:{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride
CAS No.:181725-65-5
Molecular Formula:C₅₄H₅₈Cl₂N₂O₁₁
Molecular Weight:981.967
Hs Code.:

{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Synonyms:{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Suppliers and Price of {2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of {2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of {2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

There total 13 articles about {2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24878-25-9
bis(2-aminophenyl)ether

: 181725-65-5
{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Guidance literature:: Multi-step reaction with 7 steps

1: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

2: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

3: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

4: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

5: 81 percent / Et₄NBr, aq. NaOH / CH₂Cl₂ / 72 h

6: 100 percent / CF₃CO₂H / CH₂Cl₂ / 72 h

7: (COCl)2, DMF / CH₂Cl₂ / 16 h / Ambient temperature

With sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; tetraethylammonium bromide; hydrogen; sodium hydride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-1996-4319

Reference yield:

: 2217-65-4
bis(2-nitrophenyl)ether

: 181725-65-5
{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / NH₂NH₂*H₂O / 10percent Pd/C / ethanol / 1 h / Heating

2: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

3: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

4: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

5: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

6: 81 percent / Et₄NBr, aq. NaOH / CH₂Cl₂ / 72 h

7: 100 percent / CF₃CO₂H / CH₂Cl₂ / 72 h

8: (COCl)2, DMF / CH₂Cl₂ / 16 h / Ambient temperature

With sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; tetraethylammonium bromide; hydrogen; sodium hydride; hydrazine hydrate; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-1996-4319

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 181725-65-5
{2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-chlorocarbonylmethoxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-acetyl chloride

Guidance literature:: Multi-step reaction with 9 steps

1: 77 percent / K₂CO₃ / dimethylsulfoxide / 16 h / 95 °C

2: 80 percent / NH₂NH₂*H₂O / 10percent Pd/C / ethanol / 1 h / Heating

3: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

4: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

5: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

6: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

7: 81 percent / Et₄NBr, aq. NaOH / CH₂Cl₂ / 72 h

8: 100 percent / CF₃CO₂H / CH₂Cl₂ / 72 h

9: (COCl)2, DMF / CH₂Cl₂ / 16 h / Ambient temperature

With sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; tetraethylammonium bromide; hydrogen; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1055/s-1996-4319